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Download Confined With Goddesses [v0.2.7] Walkthrough

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Download Confined with Goddesses [v0.2.7] Walkthrough

In this contribution we introduce an experimental setup to perform con-focal micro X-ray fluorescence measurements in situ in samples at high temperatures and pressures in diamond anvil cells (DAC) (e.g. Schmidt et al. 2007). The con-focal arrangement is used to suppress the background in X-ray fluorescence (XRF) spectra that stems from elastic and inelastic scattering of the diamond anvils. The setup is based on a focusing optic in the incident beam that reaches a spot of 5-10 μm and a focusing poly-capillary in front of an energy-dispersive solid-state detector. The detector poly-capillary is designed to work at a very long working distance of 50 mm in order to collect the radiation from the center of the DAC at 90 to the incident beam. The probing volume is defined by the two foci and has a size of ca. 300 μm at 8 keV and 150 μm at 19 keV as measured by scans through thin metal foils. Comparison of XRF spectra acquired with a usual detector collimator and spectra recorded with the detector capillary shows a strong suppression of XRF signal generated outside the probed volume, i.e. XRF from the gasket material and signal from elastic and Compton scattering by the diamond anvils. The ratio of the Zr K-alpha fluorescence peak to the peak of the Compton scattering changes from 0.5 (collimator) to 1.26 (detector capillary) for a ca. 1000 ppm Zr standard solution and an incident beam energy of 20 keV. For a standard solution containing ca. 1000 ppm Hf, the ratio of the L-alpha to the Compton signal increases to 6 using the detector capillary and an incident beam energy of 9.7 keV. Thus, the con-focal setup substantially improves the fluorescence to background ratio. This will result in higher sensitivities for dilute elements in the sample chamber of the DAC. Furthermore, the possibilities of interference of the sample's signal with signal from the sample environment are greatly reduced. In a broader sense, the setup can also be applied to other confined samples

Landslides in the region north of Lisbon during the last 60 years have been induced almost entirely by rainfall, and landslide activity has been confined to very wet periods. Previous results obtained using empirical relationships between rainfall intensity and slope instability show that critical rainfall conditions for failure are not the same for different types of landslides (Zêzere et al, 2008). Shallow translational soil slips have been related to intense rainfall periods ranging from 1 to 15 days, while deep slope movements (translational slides, rotational slides and complex and composite slope movements) have been occurred in relation to longer periods of less intense rain, lasting from 30 to 90 days. The different time span is consistent with the distinct hydrological triggering conditions related to different types of landslides. Intense rainfall is responsible by the rapid growth of pore pressure and by the loss of the apparent cohesion of thin soils, resulting in failure within the soil material or at the contact with the underlying impermeable bedrock. Long lasting precipitation periods allows the steady rising of the groundwater table, thus resulting in deep failures in soils and rocks by the reduction of shear strength. Rainfall information regarding 19 important landslide events occurred between 1958 and 2001, and the knowledge of the circulation weather types (CWTs) affecting those days, allow us to study the relationship between the CWTs frequency and the occurrence of landslide episodes. We have identified 10 basic CWTs (Cyclonic, Anticyclonic and 8 directional types) following the methodology previously adopted (Trigo and DaCamara, 2000). The composites and anomalies of several meteorological fields associated to landslide events show a large precipitation anomaly in the central region of Portugal and an anomalous low-pressure system located northwest of Iberia. This pattern is similar for both shallow and deep landslides events. However, for 041b061a72


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